C₂₀H₂₄OSi

Base Information

• Chemical Name: C₂₀H₂₄OSi
• CAS No.: 1440569-85-6
• Molecular Formula: C₂₀H₂₄OSi
• Molecular Weight: 308.495
• Mol file: 1440569-85-6.mol

Synonyms:C₂₀H₂₄OSi

Chemical Property of C₂₀H₂₄OSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₀H₂₄OSi

There total 1 articles about C₂₀H₂₄OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-(tert-butyldiphenylsilyl)but-3-yn-2-one (460095-28-7) → C20H24OSi (1440569-85-6)

Guidance literature:

With Ru(OTf)(TsDPEN)(η6-p-cymene); In methanol; at 50 ℃; for 15h; under 7500.75 Torr; enantioselective reaction; Autoclave;

DOI:10.1021/ol4012184

Reference yield:

C20H24OSi (1440569-85-6) → (S)-(-)-3-butyn-2-ol (2914-69-4) + (R)-(+)-3-butyn-2-ol (42969-65-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/ol4012184

upstream raw materials:

4-(tert-butyldiphenylsilyl)but-3-yn-2-one

Downstream raw materials:

(S)-(-)-3-butyn-2-ol

(R)-(+)-3-butyn-2-ol

Refernces