Technology Process of 9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole
There total 5 articles about 9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
dichloromethane;
at 20 ℃;
DOI:10.1039/c2jm30742a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dibenzo-18-crown-6; copper; potassium carbonate / 1,2-dichloro-benzene / 12 h / 100 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: dihydrogen peroxide / dichloromethane / 20 °C
With
dibenzo-18-crown-6; n-butyllithium; dihydrogen peroxide; copper; potassium carbonate;
In
tetrahydrofuran; hexane; dichloromethane; 1,2-dichloro-benzene;
1.1: Ullmann reaction;
DOI:10.1039/c2jm30742a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: dihydrogen peroxide / dichloromethane / 20 °C
With
n-butyllithium; dihydrogen peroxide;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c2jm30742a