12,13-diolbakuchiol

Base Information

• Chemical Name: 12,13-diolbakuchiol
• CAS No.: 1026776-43-1
• Molecular Formula: C₁₈H₂₆O₃
• Molecular Weight: 290.403
• Mol file: 1026776-43-1.mol

Synonyms:12,13-diolbakuchiol

Chemical Property of 12,13-diolbakuchiol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 12,13-diolbakuchiol

There total 1 articles about 12,13-diolbakuchiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

bakuchiol (17015-60-0,93998-10-8,10309-37-2) → 12,13-diolbakuchiol (1026776-43-1)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; water; at 25 ℃; for 0.0166667h;

DOI:10.1016/j.bmc.2007.11.054

Reference yield: 80.0%

12,13-diolbakuchiol (1026776-43-1) → C15H18O2

Guidance literature:

With sodium periodate; water; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.ejmech.2016.02.034

Reference yield: 64.0%

12,13-diolbakuchiol (1026776-43-1) → C18H24O2 (1026776-44-2) + 3-hydroxy-Δ1-bakuchiol (178765-55-4)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1016/j.bmc.2007.11.054

upstream raw materials:

bakuchiol

Downstream raw materials:

C₁₈H₂₄O₂

3-hydroxy-Δ¹-bakuchiol

Refernces

• 1、 Chen, Hongli,Du, Xiaolong,Tang, Wei,Zhou, Yu,Zuo, Jianping,Feng, Huijin,Li, Yuanchao. "Synthesis and structure-immunosuppressive activity relationships of bakuchiol and its derivatives". . p. 2403 - 2411. Retrieved 2008/09/21.