C₃₇H₃₄N₄O₆

Base Information

• Chemical Name: C₃₇H₃₄N₄O₆
• CAS No.: 195617-12-0
• Molecular Formula: C₃₇H₃₄N₄O₆
• Molecular Weight: 630.7
• Mol file: 195617-12-0.mol

Synonyms:C₃₇H₃₄N₄O₆

Chemical Property of C₃₇H₃₄N₄O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₃₄N₄O₆

There total 1 articles about C₃₇H₃₄N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C35H30N4O6 (195617-10-8) + methyl iodide (74-88-4) → C37H34N4O6 (195617-12-0)

Guidance literature:

With potassium hydroxide; tetrabutylammomium bromide;

DOI:10.1021/ja9626143

Reference yield: 96.0%

C37H34N4O6 (195617-12-0) → C36H34N4O5 (188028-11-7)

Guidance literature:

With hydrogen; platinum(IV) oxide;

DOI:10.1021/ja9626143

Reference yield:

C37H34N4O6 (195617-12-0) → staurosporine (62996-74-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 79 mg / H₂ / PtO₂ / aq. acetic acid

2: 2.) BH₃*DMS / 1) THF; 2) THF, toluene, reflux, 2 h

3: 70 percent / TFA, anisole / 48 h

With dimethylsulfide borane complex; hydrogen; methoxybenzene; trifluoroacetic acid; platinum(IV) oxide; In acetic acid;

DOI:10.1021/ja971304x

upstream raw materials:

C₃₅H₃₀N₄O₆

methyl iodide

Downstream raw materials:

C₃₆H₃₄N₄O₅

staurosporine

C₃₇H₃₆N₄O₅

Refernces

• 1、 Wood, John L.,Stoltz, Brian M.,Goodman, Steven N.. "Total synthesis of (+)-RK-286c, (+)-MLR-52, (+)-staurosporine, and (+)-K252a". . p. 10656 - 10657. Retrieved 2007/10/03.