Technology Process of (S)-(-)-zearalenone dimethyl ether ethylene glycol
There total 1 articles about (S)-(-)-zearalenone dimethyl ether ethylene glycol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetic acid / ethanol / Reflux
2.1: n-butyllithium / tetrahydrofuran / 0 °C
2.2: 0 °C
3.1: toluene-4-sulfonic acid / benzene / 80 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran
5.1: potassium hexamethylsilazane / tetrahydrofuran / 0 °C
6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 80 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran; ethanol; toluene; benzene;
DOI:10.1016/j.bmc.2013.06.024
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
water; acetone;
at 40 ℃;
for 26h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / water; acetone / 40 °C
2: aluminium(III) iodide; tetra-(n-butyl)ammonium iodide; 3,5-dihydroxyphenol / benzene / 5 °C
With
aluminium(III) iodide; 3,5-dihydroxyphenol; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid;
In
water; acetone; benzene;
DOI:10.1016/j.bmc.2013.06.024
