1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester

Base Information

• Chemical Name: 1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester
• CAS No.: 1231747-40-2
• Molecular Formula: C₂₆H₃₃NO₂S
• Molecular Weight: 423.62
• Mol file: 1231747-40-2.mol

Synonyms:1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester

Chemical Property of 1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester

There total 1 articles about 1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-aminonaphthalene-2-thiol (63512-54-9) + 1-methyl-1-cyclohexancarboxylic acid chloride (2890-61-1) → 1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester (1231747-40-2)

Guidance literature:

With pyridine; at 20 - 60 ℃;

Reference yield:

1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester (1231747-40-2) → 1-methyl-cyclohexanecarboxylic acid(2-mercapto-naphthalen-1-yl)-amide (1231747-38-8)

Guidance literature:

1-methyl-cyclohexanecarbothioic acid S-{1-[(1-methyl-cyclohexanecarbonyl)-amino]-naphthalen-2-yl}ester; With potassium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

With potassium hydrogensulfate; In water;

upstream raw materials:

1-aminonaphthalene-2-thiol

1-methyl-1-cyclohexancarboxylic acid chloride

Downstream raw materials:

1-methyl-cyclohexanecarboxylic acid(2-mercapto-naphthalen-1-yl)-amide

Refernces