Technology Process of C16H12ClNO3S
There total 4 articles about C16H12ClNO3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; pyridine N-oxide; oxygen; copper diacetate;
In
dichloromethane;
at 20 ℃;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium ethanolate / N,N-dimethyl-formamide / 0.5 h / 0 °C
1.2: 120 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
3.1: acetic anhydride / Reflux
3.2: 4 h / 20 °C
4.1: copper diacetate; pyridine N-oxide; pyridine; oxygen / dichloromethane / 20 °C / Molecular sieve
With
pyridine; pyridine N-oxide; oxygen; sodium ethanolate; copper diacetate; acetic anhydride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
2.1: acetic anhydride / Reflux
2.2: 4 h / 20 °C
3.1: copper diacetate; pyridine N-oxide; pyridine; oxygen / dichloromethane / 20 °C / Molecular sieve
With
pyridine; pyridine N-oxide; oxygen; copper diacetate; acetic anhydride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;