Technology Process of C18H13BrN4O3
There total 3 articles about C18H13BrN4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C11H8BrN3O;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
for 0.5h;
1-bromomethyl-4-nitro-benzene;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
DOI:10.1016/j.ejmech.2012.09.001
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: polyphosphoric acid / 3 h / 85 °C
2.1: aluminum (III) chloride / dichloromethane / 3 h / Inert atmosphere; Reflux
3.1: hydrazine hydrate / ethanol / 22 h / 20 °C / Reflux
4.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / 20 °C
4.2: 20 °C
With
aluminum (III) chloride; sodium hydride; hydrazine hydrate;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2012.09.001
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / dichloromethane / 3 h / Inert atmosphere; Reflux
2.1: hydrazine hydrate / ethanol / 22 h / 20 °C / Reflux
3.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / 20 °C
3.2: 20 °C
With
aluminum (III) chloride; sodium hydride; hydrazine hydrate;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2012.09.001