2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoyl Fluoride

Base Information

• Chemical Name: 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoyl Fluoride
• CAS No.: 5927-65-1
• Molecular Formula: C7HF13O
• Molecular Weight: 348.06
• Hs Code.: 2915900090
• DSSTox Substance ID: DTXSID70379831
• Wikidata: Q82169826
• Mol file: 5927-65-1.mol

Synonyms:7H-Perfluoroheptanoyl fluoride;5927-65-1;2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoyl Fluoride;7H-Dodecafluoroheptanoyl fluoride;DTXSID70379831;MFCD00155774;AKOS016015547;FT-0621418;A832235

Chemical Property of 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoyl Fluoride

Chemical Property:

• Vapor Pressure: 13.4mmHg at 25°C
• Refractive Index: 1.272
• Boiling Point: 91°C
• Flash Point: 40°C
• PSA: 17.07000
• Density: 1.636g/cm³
• LogP: 3.92410
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 14
• Rotatable Bond Count: 6
• Exact Mass: 347.9819808
• Heavy Atom Count: 21
• Complexity: 411

Purity/Quality:

98%Min ^*data from raw suppliers

7H-PerfluoroheptanoylFluoride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 34
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(C(C(C(C(C(=O)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F

Technology Process of 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoyl Fluoride

There total 3 articles about 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoyl Fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7,H-dodecafluoroheptanoyl chloride (41405-35-0) → Perfluoro-7-hydroheptaldehyd (5927-65-1)

Guidance literature:

With sodium fluoride; In diethylene glycol dimethyl ether; Heating;

DOI:10.1021/jo00445a014

Reference yield:

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoic acid (1546-95-8) → Perfluoro-7-hydroheptaldehyd (5927-65-1)

Guidance literature:

Multi-step reaction with 2 steps

1: PhCOCl

2: NaF / bis-(2-methoxy-ethyl) ether / Heating

With benzoyl chloride; sodium fluoride; In diethylene glycol dimethyl ether;

DOI:10.1021/jo00445a014

Reference yield:

→ Perfluoro-7-hydroheptaldehyd (5927-65-1)

Guidance literature:

1,1,7-Hydroperfluoroheptanol, Na-Dichromat, H2SO4;

upstream raw materials:

7,H-dodecafluoroheptanoyl chloride

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoic acid