1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine

Base Information

• Chemical Name: 1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine
• CAS No.: 126661-09-4
• Molecular Formula: C₅H₁₃N₃*C₇H₆N₂O₄
• Molecular Weight: 297.314
• Mol file: 126661-09-4.mol

Synonyms:1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine

Chemical Property of 1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine

There total 2 articles about 1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-nitro-4-(nitromethyl)benzene (1610-26-0) + N,N,N',N'-tetramethylguanidine (80-70-6) → 1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine (126661-09-4)

Guidance literature:

In 1,3,5-trimethyl-benzene; at 30 ℃; Equilibrium constant; Rate constant; Irradiation; other solvents;

DOI:10.1021/ja00423a037

Reference yield:

1-nitro-4-(nitromethyl)benzene (1610-26-0) + N,N,N',N'-tetramethylguanidine (80-70-6) → C7H5N2O4(1-)*C5H13N3*H(1+) (126661-09-4)

Guidance literature:

In toluene; at 25 ℃; under 750060 Torr; Rate constant; further solvents, equilibrium;

DOI:10.1246/cl.1980.887

Reference yield:

1-Nitro-4-nitromethyl-benzene; compound with N,N,N',N'-tetramethyl-guanidine (126661-09-4) → 1-nitro-4-(nitromethyl)benzene (1610-26-0) + N,N,N',N'-tetramethylguanidine (80-70-6)

Guidance literature:

In 1,3,5-trimethyl-benzene; at 30 ℃; Equilibrium constant; Irradiation; other solvents;

DOI:10.1021/ja00423a037

upstream raw materials:

1-nitro-4-(nitromethyl)benzene

N,N,N',N'-tetramethylguanidine

Downstream raw materials:

1-nitro-4-(nitromethyl)benzene

N,N,N',N'-tetramethylguanidine

Refernces

• 1、 Hubbard,C.D. et al.. "-". . p. 1870 - 1875. Retrieved 1976.