3-ETHYL-2-METHYLBENZOTHIAZOLIUM PERCHLORATE

Base Information

• Chemical Name: 3-ETHYL-2-METHYLBENZOTHIAZOLIUM PERCHLORATE
• CAS No.: 50378-33-1
• Molecular Formula: C₂₆H₂₈O₆
• Molecular Weight: 436.505
• Hs Code.: 2918300090
• Mol file: 50378-33-1.mol

Synonyms:3-ETHYL-2-METHYLBENZOTHIAZOLIUM PERCHLORATE

Chemical Property of 3-ETHYL-2-METHYLBENZOTHIAZOLIUM PERCHLORATE

Chemical Property:

• Melting Point: 140.5 °C
• PSA: 106.39000
• LogP: 2.73140

Purity/Quality:

99%min ^*data from raw suppliers

3-ETHYL-2-METHYLBENZOTHIAZOLIUM PERCHLORATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ETHYL-2-METHYLBENZOTHIAZOLIUM PERCHLORATE

There total 2 articles about 3-ETHYL-2-METHYLBENZOTHIAZOLIUM PERCHLORATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl 1,4-cyclohexanedione-2,5-dicarboxylate (787-07-5) + iodomethylbenzene (620-05-3) → trans-2,5-bis(ethoxycarbonyl)-2,5-dibenzylcyclohexane-1,4-dione (50378-33-1) + cis-2,5-bis(ethoxycarbonyl)-2,5-dibenzylcyclohexane-1,4-dione (50378-31-9,50378-33-1)

Guidance literature:

With potassium carbonate; In acetone; Yield given. Yields of byproduct given; Heating;

DOI:10.1021/jo00243a017

Reference yield:

diethyl 1,4-cyclohexanedione-2,5-dicarboxylate (787-07-5) + iodomethylbenzene (620-05-3) → trans-2,5-bis(ethoxycarbonyl)-2,5-dibenzylcyclohexane-1,4-dione (50378-33-1) + cis-2,5-bis(ethoxycarbonyl)-2,5-dibenzylcyclohexane-1,4-dione (50378-31-9,50378-33-1)

Guidance literature:

With potassium carbonate; In acetone; Yield given. Yields of byproduct given; Heating;

DOI:10.1021/jo00243a017

Reference yield: 94.0%

2,5-bis(ethoxycarbonyl)-2,5-dibenzylcyclohexane-1,4-dione (50378-31-9,50378-33-1) → trans-2,5-dibenzylcyclohexane-1,4-dione (50378-38-6)

Guidance literature:

With sulfuric acid; In ethanol; for 60h; Heating;

DOI:10.1021/jo00243a017

upstream raw materials:

diethyl 1,4-cyclohexanedione-2,5-dicarboxylate

iodomethylbenzene

Downstream raw materials:

trans-2,5-dibenzylcyclohexane-1,4-dione

trans-1,4-bis(dicyanomethylene)-2,5-dibenzylcyclohexane

Refernces