benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate

Base Information

• Chemical Name: benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate
• CAS No.: 1186663-59-1
• Molecular Formula: C₃₀H₂₈O₄S
• Molecular Weight: 484.616
• Mol file: 1186663-59-1.mol

Synonyms:benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate

Chemical Property of benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate

Chemical Property:

Purity/Quality:

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Technology Process of benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate

There total 1 articles about benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

S-(4,4'-dimethoxytrityl)mercaptoacetic acid (1186663-56-8) + benzyl alcohol (100-51-6,185532-71-2) → benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate (1186663-59-1)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; diisopropyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere; Cooling with ice;

DOI:10.1002/ejoc.200900271

Reference yield: 80.0%

benzyl S-(4,4'-dimethoxytrityl)mercaptoacetate (1186663-59-1) → mercaptoacetic acid benzyl ester (7383-63-3)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/ejoc.200900271

upstream raw materials:

S-(4,4'-dimethoxytrityl)mercaptoacetic acid

benzyl alcohol

Downstream raw materials:

mercaptoacetic acid benzyl ester

Refernces