CHOLESTEROL-3-D1

Base Information

• Chemical Name: CHOLESTEROL-3-D1
• CAS No.: 51467-57-3
• Molecular Formula: C27H45DO
• Molecular Weight: 387.66
• Mol file: 51467-57-3.mol

Synonyms:CHOLESTEROL-3-D1;Cholesterol-d1

Chemical Property of CHOLESTEROL-3-D1

Chemical Property:

• Boiling Point: 480.648 °C at 760 mmHg
• Flash Point: 209.291 °C
• PSA: 20.23000
• Density: 0.99 g/cm³
• LogP: 7.38870

Purity/Quality:

99% ^*data from raw suppliers

Cholesterol-3-d1 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Cholesterol-3-d1 (CAS# 51467-57-3) is a useful isotopically labeled research compound.

Technology Process of CHOLESTEROL-3-D1

There total 3 articles about CHOLESTEROL-3-D1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

Cholest-5-en-3-one (601-54-7) → 3-2H-cholesterol (51467-57-3)

Guidance literature:

With sodium borodeuteride; In methanol; chloroform; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2015.05.014

Reference yield:

Cholest-5-en-3-one (601-54-7) → epicholesterol-3β-d1 (98936-76-6) + 3-2H-cholesterol (51467-57-3)

Guidance literature:

With lithium aluminium deuteride; diethyl ether;

Reference yield:

→ 3α-d(1)-Cholesterin (51467-57-3,98936-76-6)

Guidance literature:

Cholesteron, LiAlH4;

DOI:10.1021/bi00607a006

upstream raw materials:

Cholest-5-en-3-one

Refernces

• 1、 Cui, Jin,Matsuoka, Shigeru,Kinoshita, Masanao,Matsumori, Nobuaki,Sato, Fuminori,Murata, Michio,Ando, Jun,Yamakoshi, Hiroyuki,Dodo, Kosuke,Sodeoka, Mikiko. "Novel Raman-tagged sphingomyelin that closely mimics original raft-forming behavior". supporting information. p. 2989 - 2994. Retrieved 2015/08/03.
• 2、 Oldfield,Meadows,Rice,Jacobs. "Spectroscopic studies of specifically deuterium labeled membrane systems. Nuclear magnetic resonance investigation of the effects of cholesterol in model systems". . p. 2727 - 2740,2735, 2736, 2737. Retrieved 2007/10/14.