2-phenyl-4,5-tridecamethylenepyrazolone

Base Information Edit

Chemical Name:2-phenyl-4,5-tridecamethylenepyrazolone
CAS No.:75446-68-3
Molecular Formula:C₂₂H₃₂N₂O
Molecular Weight:340.509
Hs Code.:
Mol file:75446-68-3.mol

Synonyms:2-phenyl-4,5-tridecamethylenepyrazolone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl-4,5-tridecamethylenepyrazolone Edit

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Technology Process of 2-phenyl-4,5-tridecamethylenepyrazolone

There total 2 articles about 2-phenyl-4,5-tridecamethylenepyrazolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 5682-97-3,58643-76-8
ethyl 2-oxocyclopentadecanecarboxylate

: 100-63-0
phenylhydrazine

: 75446-68-3
2-phenyl-4,5-tridecamethylenepyrazolone

Guidance literature:: In toluene; 1) 90 deg C, 2 h 2) 130 deg C, 3 h;
DOI:10.1007/BF00557742

Reference yield:

: 20894-58-0
2-carbethoxy-<11>-α-cyclothien-1-one

: 75446-68-3
2-phenyl-4,5-tridecamethylenepyrazolone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / hydrogen / Raney nickel / ethanol; acetone / 3 h / 20 °C

2: 79 percent / toluene / 1) 90 deg C, 2 h 2) 130 deg C, 3 h

With hydrogen; nickel; In ethanol; acetone; toluene;
DOI:10.1007/BF00557742