2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid

Base Information

• Chemical Name: 2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid
• CAS No.: 1389396-43-3
• Molecular Formula: C₁₀H₇N₅O₉S
• Molecular Weight: 373.26
• Mol file: 1389396-43-3.mol

Synonyms:2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid

Chemical Property of 2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid

There total 1 articles about 2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

BARBITURIC ACID (67-52-7,944357-77-1) + 2-hydroxy-3-amino-5-nitrobenzenesulfonic acid (96-67-3) → 2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid (1389396-43-3)

Guidance literature:

2-hydroxy-3-amino-5-nitrobenzenesulfonic acid; With hydrogenchloride; sodium hydroxide; sodium nitrite; In water; at -0.16 ℃;

BARBITURIC ACID; In water; at -0.16 ℃; for 1h;

DOI:10.1016/j.ejmech.2019.01.021

Reference yield: 48.0%

2-hydroxy-5-nitro-3-(2-(2,4,6-trioxotetrahydro-pyrimidin-5(2H)-ylidene)hydrazinyl)benzene sulfonic acid (1389396-43-3) + water (7732-18-5) + copper(II) nitrate + sodium hydroxide (1310-73-2) → [CuNa(H2O)2(η9-2-hydroxy-5-nitro-3-(2-(2,4,6-trioxatetrahydropyrimidin-5(2H)ylidene)hydrazinyl)benzene sulfonic acid(-3H))]..

Guidance literature:

In water; stoich. mixt. stirred for 5 min; crystd. in 2 d;

DOI:10.1016/j.inoche.2012.06.008

upstream raw materials:

BARBITURIC ACID

2-hydroxy-3-amino-5-nitrobenzenesulfonic acid

Refernces