Technology Process of 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)
There total 4 articles about 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin; magnesium bromide;
In
dichloromethane;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
- Guidance literature:
-
With
triethylamine; magnesium bromide;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1039/c2cc30591g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 9 h / 20 °C / Inert atmosphere
2: triethylamine; magnesium bromide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
With
triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; magnesium bromide;
In
dichloromethane;
DOI:10.1039/c2cc30591g