(3,5-dimethoxybenzyl)trimethylammonium chloride

Base Information

• Chemical Name: (3,5-dimethoxybenzyl)trimethylammonium chloride
• CAS No.: 26050-72-6
• Molecular Formula: C₁₂H₂₀NO₂*Cl
• Molecular Weight: 245.749
• Mol file: 26050-72-6.mol

Synonyms:(3,5-dimethoxybenzyl)trimethylammonium chloride

Chemical Property of (3,5-dimethoxybenzyl)trimethylammonium chloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (3,5-dimethoxybenzyl)trimethylammonium chloride

There total 1 articles about (3,5-dimethoxybenzyl)trimethylammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethoxybenzylchloride (6652-32-0) + trimethylamine (75-50-3) → (3,5-dimethoxybenzyl)trimethylammonium chloride (26050-72-6)

Guidance literature:

In acetonitrile;

DOI:10.1021/jo01351a039

Reference yield:

methanol (67-56-1) + (3,5-dimethoxybenzyl)trimethylammonium chloride (26050-72-6) → 1,3-dimethoxy-5-methylbenzene (4179-19-5) + 1-methylmethoxy-3,5-dimethoxybenzene (73569-69-4) + N,N-dimethylammonium chloride (506-59-2) + trimethylamine hydrochloride (593-81-7)

Guidance literature:

at 30 ℃; for 2h; Irradiation;

Reference yield:

methanol (67-56-1) + (3,5-dimethoxybenzyl)trimethylammonium chloride (26050-72-6) → 3,5,3',5'-tetramethoxy-bibenzyl (22976-41-6) + 1,3-dimethoxy-5-methylbenzene (4179-19-5) + 3,5-dimethoxyphenethyl alcohol (7417-20-1) + 1-methylmethoxy-3,5-dimethoxybenzene (73569-69-4)

Guidance literature:

at 25 ℃; Product distribution; Photolysis;

DOI:10.1021/jo000387o

upstream raw materials:

3,5-dimethoxybenzylchloride

trimethylamine

Downstream raw materials:

N,N-Dimethyl-2,4-dimethoxy-6-methylbenzylamine

1,3-dimethoxy-5-methylbenzene

1-methylmethoxy-3,5-dimethoxybenzene

N,N-dimethylammonium chloride

Refernces

• 1、 DeCosta,Howell,Pincock,Pincock,Rifai. "1,3-Dimethoxy-5-methylene-1,3-cyclohexadiene Compounds with Leaving Groups at C6: Generation, Solvolytic Reactivity, and Their Importance in the Photochemistry of 3,5-Dimethoxybenzyl Derivatives". . p. 4698 - 4705. Retrieved 2007/10/03.