Technology Process of 6H-Furo[3,2-d]-1,3-dioxin-6-one,4a-ethoxytetrahydro-2,2-dimethyl-,(4aR,7aR)-(9CI)
There total 6 articles about 6H-Furo[3,2-d]-1,3-dioxin-6-one,4a-ethoxytetrahydro-2,2-dimethyl-,(4aR,7aR)-(9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4 A molecular sieve; toluene-4-sulfonic acid;
In
benzene;
for 0.5h;
Heating;
DOI:10.1021/jo020151f
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 50 percent / KMnO4; DCH-18-crown-6 / CH2Cl2
2: 96 percent / 4 Angstroem molecular sieves; TsOH / benzene / 0.5 h / Heating
3: 92 percent / ethylene glycol; SmI2 / tetrahydrofuran / 0.5 h / 20 °C
4: 100 percent / H2 / 10percent Pd/C / ethanol / 1 h / 760.05 Torr
5: 59 percent / 4 Angstroem molecular sieves; TsOH / benzene / 0.5 h / Heating
With
perhydrodibenzo-18-crown-6; potassium permanganate; samarium diiodide; 4 A molecular sieve; hydrogen; toluene-4-sulfonic acid; ethylene glycol;
10percent Pd/C;
In
tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1021/jo020151f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / 4 Angstroem molecular sieves; TsOH / benzene / 0.5 h / Heating
2: 92 percent / ethylene glycol; SmI2 / tetrahydrofuran / 0.5 h / 20 °C
3: 100 percent / H2 / 10percent Pd/C / ethanol / 1 h / 760.05 Torr
4: 59 percent / 4 Angstroem molecular sieves; TsOH / benzene / 0.5 h / Heating
With
samarium diiodide; 4 A molecular sieve; hydrogen; toluene-4-sulfonic acid; ethylene glycol;
10percent Pd/C;
In
tetrahydrofuran; ethanol; benzene;
DOI:10.1021/jo020151f