3,4-Dichlorophenylacetone

Base Information

• Chemical Name: 3,4-Dichlorophenylacetone
• CAS No.: 6097-32-1
• Molecular Formula: C9H8Cl2O
• Molecular Weight: 203.068
• Hs Code.: 29147000
• Mol file: 6097-32-1.mol

Synonyms:2-Propanone,(3,4-dichlorophenyl)- (7CI);

Chemical Property of 3,4-Dichlorophenylacetone

Chemical Property:

• Appearance/Colour: clear light yellow liquid
• Vapor Pressure: 0.00649mmHg at 25°C
• Refractive Index: 1.551-1.553
• Boiling Point: 271.3 °C at 760 mmHg
• Flash Point: 112.5 °C
• PSA: 17.07000
• Density: 1.27 g/cm³
• LogP: 3.12490
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

3,4-Dichlorophenylacetone ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-Dichlorophenylacetone

There total 2 articles about 3,4-Dichlorophenylacetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nitroethane (79-24-3) + 3,4-dichlorobenzaldehyde (6287-38-3) → 1-(3,4-dichlorophenyl)propanone (6097-32-1)

Guidance literature:

Multistep reaction; (i) nBuNH₂, toluene, (ii) Fe, FeCl₃, aq. HCl;

Reference yield:

→ 1-(3,4-dichlorophenyl)propanone (6097-32-1)

Guidance literature:

Reference yield: 99.0%

1-(3,4-dichlorophenyl)propanone (6097-32-1) → 2-bromo-3’,4’-dichlorophenylacetone

Guidance literature:

With N-Bromosuccinimide; toluene-4-sulfonic acid; In ethyl acetate; at 60 - 80 ℃; for 6h;

upstream raw materials:

Nitroethane

3,4-dichlorobenzaldehyde

Downstream raw materials:

2-(3,4-Dichlorphenyl)-3-butanon

1,3-Dibromo-1-(3,4-dichloro-phenyl)-propan-2-one

3-(tert-Butylamino-methyl)-3',4'-dichloro-5-(7-chloro-quinolin-4-ylamino)-biphenyl-2-ol

3',4'-Dichloro-5-(7-chloro-quinolin-4-ylamino)-3-diethylaminomethyl-biphenyl-2-ol

Refernces