2-Chloroethyl cyclohexyl sulphide

Base Information

• Chemical Name: 2-Chloroethyl cyclohexyl sulphide
• CAS No.: 53787-05-6
• Molecular Formula: C8H15ClS
• Molecular Weight: 178.72
• Hs Code.: 2930909090
• Mol file: 53787-05-6.mol

Synonyms:Cyclohexane, [(2-chloroethyl)thio]-;

Chemical Property of 2-Chloroethyl cyclohexyl sulphide

Chemical Property:

• Vapor Pressure: 0.02mmHg at 25°C
• Refractive Index: 1.504
• Boiling Point: 259.997 °C at 760 mmHg
• Flash Point: 109.366 °C
• PSA: 25.30000
• Density: 1.061 g/cm³
• LogP: 3.29110

Purity/Quality:

99% ^*data from raw suppliers

2-CHLOROETHYL CYCLOHEXYL SULPHIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Chloroethyl cyclohexyl sulphide

There total 5 articles about 2-Chloroethyl cyclohexyl sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(cyclohexylthio)ethanol (3778-81-2) → 1-[(2-chloroethyl)sulfanyl]cyclohexane (53787-05-6)

Guidance literature:

With hydrogenchloride; Heating;

DOI:10.1021/ja00871a021

Reference yield:

1-oxa-4-thia-spiro[4.5]decane (177-15-1) → 1-[(2-chloroethyl)sulfanyl]cyclohexane (53787-05-6)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃, LiAlH₄, Et₂O

2: aq. HCl / Heating

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; diethyl ether;

DOI:10.1021/ja00871a021

Reference yield:

Cyclohexanethiol (1569-69-3) → 1-[(2-chloroethyl)sulfanyl]cyclohexane (53787-05-6)

Guidance literature:

Multi-step reaction with 2 steps

2: aq. HCl / Heating

With hydrogenchloride;

DOI:10.1021/ja00871a021

upstream raw materials:

2-chloroethanethiol

cyclohexene

2-(cyclohexylthio)ethanol

1-oxa-4-thia-spiro[4.5]decane

Downstream raw materials:

cyclohexyl ethyl sulfide

4-amino-1-cyclohexylthioethyl-5-cyanoimidazole

5-amino-1-(2-cyclohexylthioethyl)imidazole-4-carbonitrile

7-cyclohexylthioethyl-6-methylamino-2-thioxopurine

Refernces

• 1、 Park, Hyunjin,Kwon, Eunjin,Kang, Gihaeng,Kim, Jineun,Kim, Tae Ho. "Photoluminescent copper(I) complex based on 3-(2-(cyclohexylthio) ethoxy)pyridine: Synthesis, structure, and physical properties". . p. 1163 - 1165. Retrieved 2016.