2,2-Dichloro-1,1,1-triethoxyethane

Base Information

• Chemical Name: 2,2-Dichloro-1,1,1-triethoxyethane
• CAS No.: 54567-92-9
• Molecular Formula: C8H16Cl2O3
• Molecular Weight: 231.119
• Hs Code.: 2909199090
• European Community (EC) Number: 678-322-1
• DSSTox Substance ID: DTXSID90508121
• Wikidata: Q82364832
• Mol file: 54567-92-9.mol

Synonyms:2,2-dichloro-1,1,1-triethoxyethane;54567-92-9;Triethyl Orthodichloroacetate;Orthodichloroacetic Acid Triethyl Ester;SCHEMBL4405318;DTXSID90508121;MFCD01861293;1,1,1-Triethoxy-2,2-dichloroethane;BS-23818;CS-0205176;O0274;T72599;EN300-7415303

Chemical Property of 2,2-Dichloro-1,1,1-triethoxyethane

Chemical Property:

• Refractive Index: 1.4340 to 1.4380
• Boiling Point: 195 °C
• PSA: 27.69000
• Density: 1,13 g/cm3
• LogP: 2.55340
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 7
• Exact Mass: 230.0476498
• Heavy Atom Count: 13
• Complexity: 114

Purity/Quality:

98%,99%, ^*data from raw suppliers

Triethyl Orthodichloroacetate ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(C(Cl)Cl)(OCC)OCC

Technology Process of 2,2-Dichloro-1,1,1-triethoxyethane

There total 1 articles about 2,2-Dichloro-1,1,1-triethoxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,2,2-tetrachloroethylene (127-18-4) + sodium ethanolate (141-52-6) → 1,1,2-trichloro-2-ethoxyethylene (14416-73-0) + 1,1,1-triethoxy-2,2-dichloroethane (54567-92-9) + ethyl 1,1-dichloroacetate (535-15-9)

Guidance literature:

at 100 - 120 ℃;

Reference yield: 95.0%

1,1,1-triethoxy-2,2-dichloroethane (54567-92-9) → ethanol (64-17-5) + ethyl acetate (141-78-6) + ethyl 1,1-dichloroacetate (535-15-9)

Guidance literature:

With acetic acid; Heating;

upstream raw materials:

1,1,2,2-tetrachloroethylene

sodium ethanolate

Downstream raw materials:

ethanol

ethyl acetate

ethyl 1,1-dichloroacetate