6-CHLOROHEXANAL

Base Information

• Chemical Name: 6-CHLOROHEXANAL
• CAS No.: 52387-36-7
• Molecular Formula: C6H11ClO
• Molecular Weight: 134.606
• Hs Code.: 2913000090
• Mol file: 52387-36-7.mol

Synonyms:6-CHLOROHEXANAL

Chemical Property of 6-CHLOROHEXANAL

Chemical Property:

• Boiling Point: 50-51 °C(Press: 0.5 Torr)
• PSA: 17.07000
• Density: 0.987±0.06 g/cm3(Predicted)
• LogP: 1.98450

Purity/Quality:

98%,99%, ^*data from raw suppliers

6-Chlorohexanal ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-CHLOROHEXANAL

There total 3 articles about 6-CHLOROHEXANAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanol (108-93-0) → 6-chlorohexanoic acid (4224-62-8) + 6-chlorohexanal (52387-36-7) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + hexanal (66-25-1)

Guidance literature:

With pyridine; lead(IV) acetate; lithium chloride; In benzene; at 65 - 70 ℃; for 0.25h; Further byproducts given;

DOI:10.1007/BF00948994

Reference yield:

cyclohexanol (108-93-0) → 6-chlorohexanal (52387-36-7) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4)

Guidance literature:

With lead(IV) acetate; lithium chloride; In benzene; at 80 ℃; Yield given. Yields of byproduct given;

DOI:10.1007/BF00959880

Reference yield:

cyclohexanol (108-93-0) → 2,4,6-tris(5-chloroamyl)-1,3,5-trioxane (93636-84-1) + 6-chlorohexanoic acid (4224-62-8) + 6-chlorohexanal (52387-36-7) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4)

Guidance literature:

With pyridine; lead(IV) acetate; lithium chloride; In benzene; at 65 - 70 ℃; for 0.25h; Further byproducts given;

DOI:10.1007/BF00948994

upstream raw materials:

cyclohexanol

Downstream raw materials:

3-{6-chloro-1-[(4-methylphenyl)sulfonyl]hexyl}-1H-indazole

(S)-6-chloro-1-hydroxyhexan-2-yl benzoate

vilazodone

3-(4-chlorobutyl)-5-cyanoindole

Refernces

• 1、 Nikishin, G. I.,Kapustina, N. I.. "OXIDATIVE SPLITTING OF SECONDARY CYCLOALKANOLS BY Pb(OAc)4-LiCl AND Pb(OAc)4-Cu(OAc)2 SYSTEMS". . p. 1235 - 1239. Retrieved 2007/10/02.