1,1,1-TRIFLUORO-3-IODOBUTANE

Base Information

• Chemical Name: 1,1,1-TRIFLUORO-3-IODOBUTANE
• CAS No.: 540-87-4
• Molecular Formula: C4H6F3I
• Molecular Weight: 237.991
• Hs Code.: 2903799090
• Mol file: 540-87-4.mol

Synonyms:1,1,1-TRIFLUORO-3-IODOBUTANE;3-IODO-1,1,1-TRIFLUOROBUTANE

Chemical Property of 1,1,1-TRIFLUORO-3-IODOBUTANE

Chemical Property:

• Vapor Pressure: 31.7mmHg at 25°C
• Refractive Index: 1.435
• Boiling Point: 107.4°Cat760mmHg
• Flash Point: 34.5°C
• PSA: 0.00000
• Density: 1.828g/cm³
• LogP: 2.76230

Purity/Quality:

98%Min ^*data from raw suppliers

3-Iodo-1,1,1-trifluorobutane ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1,1-TRIFLUORO-3-IODOBUTANE

There total 5 articles about 1,1,1-TRIFLUORO-3-IODOBUTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

propene (187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4) + iodotrifluoromethane (2314-97-8,263005-66-9) → 1,1,1-trifluorobutane (460-34-4) + 3-iodo-1,1,1-trifluorobutane (540-87-4) + 4,4,4-trifluorobutene (1524-26-1) + (R*)-1,1,1-trifluoro-3-iodo-2-methylpropane (26653-47-4)

Guidance literature:

at 246.9 - 306.9 ℃; under 300 Torr; Further byproducts given;

Reference yield:

propene (187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4) + iodotrifluoromethane (2314-97-8,263005-66-9) → 1,1,1-trifluorobutane (460-34-4) + 3-iodo-1,1,1-trifluorobutane (540-87-4) + 4,4,4-trifluorobutene (1524-26-1)

Guidance literature:

Rate constant; Mechanism; Kinetics; different temperatures and pressures; product yield;

Reference yield:

propene (187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4) + iodotrifluoromethane (2314-97-8,263005-66-9) → 3-iodo-1,1,1-trifluorobutane (540-87-4) + (R*)-1,1,1-trifluoro-3-iodo-2-methylpropane (26653-47-4)

Guidance literature:

at 200 ℃;

DOI:10.1039/j39700000414

upstream raw materials:

propene

iodotrifluoromethane

Downstream raw materials:

1,1,1-trifluorobutane

4,4,4-trifluorobutene

rac-(3,3,3-trifluoro-1-methyl-propylsulfanyl)-benzene

Refernces

• 1、 -. "1-Cyano-3-(fluoroalkyl)guanidines for lowering blood pressure". . . Retrieved 2008/06/13.