GLUTARALDEHYDE 2,4-DINITROPHENYLHYDRAZONE

Base Information

• Chemical Name: GLUTARALDEHYDE 2,4-DINITROPHENYLHYDRAZONE
• CAS No.: 5085-07-4
• Molecular Formula: C17H16N8O8
• Molecular Weight: 460.363
• Hs Code.: 2928000090
• European Community (EC) Number: 621-772-0
• Nikkaji Number: J566.146C
• Mol file: 5085-07-4.mol

Synonyms:GLUTARALDEHYDE 2,4-DINITROPHENYLHYDRAZONE;GLUTARALDEHYDE-DNPH;GLUTARALDEHYDE BIS(2,4-DINITROPHENYLHYDRAZONE);Glutaraldehyde 2,4-dinitrophenylhydrazone (purity);68718, GLUTARALDEHYDE 2,4-DINITROPHENYLH;GLUTARALDEHYDE BIS(2,4-DINITROPHENYL-HYD RAZONE), ENVIRONMENTAL STD, 99%;glutaraldehyde-2,4-dnph;Glutaraldehyde 2,4-dinitrophenylhydrazone, Glutaraldehyde-2,4-DNPH solution

Chemical Property of GLUTARALDEHYDE 2,4-DINITROPHENYLHYDRAZONE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 196-197 °C(lit.)
• Refractive Index: 1.691
• Boiling Point: 680.069°C at 760 mmHg
• Flash Point: 365.093°C
• PSA: 232.06000
• Density: 1.592g/cm³
• LogP: 6.22410
• Storage Temp.: 2-8°C
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 12
• Rotatable Bond Count: 8
• Exact Mass: 460.10910950
• Heavy Atom Count: 33
• Complexity: 694

Purity/Quality:

98%Min ^*data from raw suppliers

Glutaraldehydebis(2,4-dinitrophenylhydrazone)(synthetic),≥98.5%(HPLC),Analyticalstandard,forenvironmentalanalysis ≥98.5%(HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi,Xn,F
• Hazard Codes: Xi,Xn,F
• Statements: 36/37/38-36-20/21/22-11
• Safety Statements: 26-36-16-36/37

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1[N+](=O)[O-])[N+](=O)[O-])NN=CCCCC=NNC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]
• Isomeric SMILES: C1=CC(=C(C=C1[N+](=O)[O-])[N+](=O)[O-])N/N=C\CCC/C=N\NC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]
• Uses: Glutaraldehyde 2,4-dinitrophenylhydrazone is an analytical standard for environmental analysis. Dyes and metabolites.

Technology Process of GLUTARALDEHYDE 2,4-DINITROPHENYLHYDRAZONE

There total 3 articles about GLUTARALDEHYDE 2,4-DINITROPHENYLHYDRAZONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Glutaraldehyde (111-30-8,29257-65-6,79215-57-9) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → glutaraldehyde bis-(2,4-dinitro-phenylhydrazone) (5085-07-4)

Guidance literature:

DOI:10.1039/jr9370000300

Reference yield:

2-ethoxy-2,3-dihydro-4H-pyran (103-75-3) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → glutaraldehyde bis-(2,4-dinitro-phenylhydrazone) (5085-07-4)

Guidance literature:

Multistep reaction; (i) TsOH, (ii) /BRN= 615586/;

Reference yield:

→ glutaraldehyde bis-(2,4-dinitro-phenylhydrazone) (5085-07-4)

Guidance literature:

Pentandial, 2,4-DNPH (gesaett. wss. Lsg.), 2n-HCl, Raum-Temp.;

DOI:10.1021/jo01060a056

upstream raw materials:

Glutaraldehyde

(2,4-dinitro-phenyl)-hydrazine

2-ethoxy-2,3-dihydro-4H-pyran