beta-neoclovene

Base Information

• Chemical Name: beta-neoclovene
• CAS No.: 56684-96-9
• Molecular Formula: C15H24
• Molecular Weight: 204.356
• Mol file: 56684-96-9.mol

Synonyms:beta-neoclovene

Chemical Property of beta-neoclovene

Chemical Property:

• Boiling Point: 257.1±7.0 °C(Predicted)
• PSA: 0.00000
• Density: 0.94±0.1 g/cm3(Predicted)
• LogP: 4.55910

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of beta-neoclovene

There total 4 articles about beta-neoclovene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.1%

β-caryophyllene (87-44-5) → β-caryolanol (58404-89-0,82008-48-8,129445-45-0,472-97-9) + isocaryolan-8-ol (131717-65-2) + (-)-isocaryophyllene (118-65-0) + β-neoclovene (56684-96-9)

Guidance literature:

With sulfuric acid; In diethyl ether; at 0 - 20 ℃; for 0.5h; Further byproducts given;

DOI:10.1021/ja00141a009

Reference yield: 26.1%

β-caryophyllene (87-44-5) → β-caryolanol (58404-89-0,82008-48-8,129445-45-0,472-97-9) + isocaryolan-8-ol (131717-65-2) + β-neoclovene (56684-96-9) + (3aR,7aR)-3a,7a-dimethyl-4-(2-methyl-1-propenyl)-2,3,3a,6,7,7a-hexahydro-1H-indene

Guidance literature:

With sulfuric acid; In diethyl ether; at 0 - 20 ℃; for 0.5h; Yield given. Further byproducts given. Title compound not separated from byproducts;

DOI:10.1021/ja00141a009

Reference yield: 26.1%

β-caryophyllene (87-44-5) → β-caryolanol (58404-89-0,82008-48-8,129445-45-0,472-97-9) + isocaryolan-8-ol (131717-65-2) + β-neoclovene (56684-96-9) + (1Z,5Z,9S)-2,6,10,10-tetramethylbicyclo<7.2.0>undeca-1,5-diene

Guidance literature:

With sulfuric acid; In diethyl ether; at 0 - 20 ℃; for 0.5h; Yield given. Further byproducts given. Title compound not separated from byproducts;

DOI:10.1021/ja00141a009

upstream raw materials:

β-caryophyllene

Downstream raw materials:

4-Bromo-benzoic acid (1R,2S,2aR,4aR,7aS,7bR)-2-hydroxy-2,2a,4a,7a-tetramethyl-decahydro-cyclopenta[cd]inden-1-yl ester

Refernces