Hydrazinecarboxylic acid, butyl ester

Base Information

• Chemical Name: Hydrazinecarboxylic acid, butyl ester
• CAS No.: 52709-73-6
• Molecular Formula: C5H12N2O2
• Molecular Weight: 132.16
• Mol file: 52709-73-6.mol

Synonyms:Hydrazinecarboxylic acid, butyl ester

Chemical Property of Hydrazinecarboxylic acid, butyl ester

Chemical Property:

• Boiling Point: 100 - 105 °C (9 mmHg)
• PSA: 64.35000
• LogP: 1.47760

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydrazinecarboxylic acid, butyl ester

There total 3 articles about Hydrazinecarboxylic acid, butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-butylhydrazine monohydrochloride (56795-65-4,70629-61-7) → L-butoxycarbonylhydrazine (52709-73-6)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water;

Reference yield:

imidazole-1-carboxylic acid butyl ester (83395-36-2) → L-butoxycarbonylhydrazine (52709-73-6)

Guidance literature:

With hydrazine hydrate; In dichloromethane; at 0 - 20 ℃; for 1h;

DOI:10.1002/ejoc.202000530

Reference yield:

→ L-butoxycarbonylhydrazine (52709-73-6)

Guidance literature:

EtOCO2Bu, N2H4*H2O/EtOH, Reflux;

upstream raw materials:

N-butylhydrazine monohydrochloride

imidazole-1-carboxylic acid butyl ester

Downstream raw materials:

butyl 2-(pyridin-2-yl)benzoate

Refernces

• 1、 -. "Organic hydrazine derivatives for pharmaceutical use". . . Retrieved 2008/06/13.