PICOLINIC ACID SODIUM SALT

Base Information

• Chemical Name: PICOLINIC ACID SODIUM SALT
• CAS No.: 57665-05-1
• Molecular Formula: C6H4NNaO2
• Molecular Weight: 145.093
• Hs Code.: 2933399090
• Mol file: 57665-05-1.mol

Synonyms:SODIUM PICOLINATE;SODIUM PYRIDINE-2-CARBOXYLATE;PYRIDINE-2-CARBOXYLIC ACID SODIUM SALT;PICOLINIC ACID SODIUM SALT;2-pyridinecarboxylicacid,sodiumsalt

Chemical Property of PICOLINIC ACID SODIUM SALT

Chemical Property:

• Refractive Index: 1.57
• Boiling Point: 292.5°Cat760mmHg
• Flash Point: 130.7°C
• PSA: 53.02000
• Density: 1.293g/cm³
• LogP: -0.55490
• Water Solubility.: Completely soluble in water

Purity/Quality:

98%,99%, ^*data from raw suppliers

Sodium Pyridine-2-carboxylate >98.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PICOLINIC ACID SODIUM SALT

There total 3 articles about PICOLINIC ACID SODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

2-pyridyl(3-methyl-[1,2,3] triazolo[1,5-a]pyridin-7-yl)methanol → 3-methyl-6,7-dihydro[1,2,3]triazolo[1,5-a]pyridine (1214990-35-8) + sodium picolinate (57665-05-1)

Guidance literature:

With water; sodium hydroxide; In ethanol; at 95 ℃; for 24h;

Reference yield: 28.0%

phenyl(3-phenyl-[1,2,3]triazolo[1,5-a]pyridin-7-yl)methanol (1214990-33-6) → sodium picolinate (57665-05-1) + 3-phenyl-6,7-dihydro[1,2,3]triazolo[1,5-a]pyridine

Guidance literature:

With water; sodium hydroxide; In ethanol; at 95 ℃; for 24h;

Reference yield:

2-Cyanopyridine (100-70-9,1232006-36-8) → sodium picolinate (57665-05-1)

Guidance literature:

With sodium hydroxide; In ethanol; at 78 ℃; for 1h; Temperature; Reagent/catalyst; Solvent;

upstream raw materials:

phenyl(3-phenyl-[1,2,3]triazolo[1,5-a]pyridin-7-yl)methanol

2-Cyanopyridine

Downstream raw materials:

V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2^(1-)*N(C₂H₅)4⁽¹⁺⁾=(N(C₂H₅)4)[V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2]

sodium chloride

pyridine-2-carboxylic acid amide

Refernces

• 1、 Abarca, Belen,Adam, Rosa,Ballesteros, Rafael. "Triazolopyridines. Part 27.1 the preparation of novel 6,7-dihydro[1,2,3] triazolo[1,5-a]pyridines". experimental part. p. 319 - 327. Retrieved 2010/08/19.