3-Butenyltriethoxysilane

Base Information Edit

Chemical Name:3-Butenyltriethoxysilane
CAS No.:57813-67-9
Molecular Formula:C10H22O3Si
Molecular Weight:218.368
Hs Code.:
DSSTox Substance ID:DTXSID10451746
Nikkaji Number:J1.224.764H
Wikidata:Q82271937
Mol file:57813-67-9.mol

Synonyms:3-BUTENYLTRIETHOXYSILANE;57813-67-9;but-3-enyl(triethoxy)silane;Silane, 3-butenyltriethoxy-;but-3-en-1-yltriethoxysilane;3-Butenyltriethoxysilane, 95%;vinylethyltriethoxysilane;3-butenyl triethoxysilane;but-3-enyltriethoxysilane;SCHEMBL80912;DTXSID10451746;LUZRKMGMNFOSFZ-UHFFFAOYSA-N;MFCD00069150;FT-0699509

Suppliers and Price of 3-Butenyltriethoxysilane

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 20 raw suppliers

Chemical Property of 3-Butenyltriethoxysilane Edit

Chemical Property:

Vapor Pressure:0.364mmHg at 25°C
Melting Point:-80 °C
Refractive Index:1.423
Boiling Point:205.1 °C at 760 mmHg
Flash Point:76.1 °C
PSA：27.69000
Density:0.896 g/cm³
LogP:2.61090
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:218.13382109
Heavy Atom Count:14
Complexity:133

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCO[Si](CCC=C)(OCC)OCC

Technology Process of 3-Butenyltriethoxysilane

There total 4 articles about 3-Butenyltriethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.3%

: 5162-44-7
1-bromo-4-butene

: 64-17-5
ethanol

: 57813-67-9
but-3-enyltriethoxysilane

Guidance literature:: 1-bromo-4-butene; With magnesium; In tetrahydrofuran; Inert atmosphere; Reflux;

With tetrachlorosilane; In tetrahydrofuran; at 0 - 20 ℃; for 30h; Inert atmosphere;

ethanol; With triethylamine; In tetrahydrofuran; at 0 - 23 ℃; for 24h;

Reference yield:

: 998-30-1
Triethoxysilane

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: 57813-67-9
but-3-enyltriethoxysilane

: 13436-82-3
2-butenyltriethoxysilane

Guidance literature:: With trans-{Pt(tri-tert-butylphosphine)Cl}2; methylmagnesium chloride; In tetrahydrofuran; dichloromethane; at -45 - 50 ℃; Reagent/catalyst; Solvent; Overall yield = 85 %; Overall yield = 10.2 g; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1021/ja5008596