O-(2-Methyl-allyl)-hydroxylamine hydrochloride

Base Information

• Chemical Name: O-(2-Methyl-allyl)-hydroxylamine hydrochloride
• CAS No.: 54149-64-3
• Molecular Formula: C4H10ClNO
• Molecular Weight: 123.582
• Hs Code.: 2922199090
• DSSTox Substance ID: DTXSID00500474
• Mol file: 54149-64-3.mol

Synonyms:54149-64-3;O-(2-Methyl-allyl)-hydroxylamine hydrochloride;O-(2-methylallyl)hydroxylamine hydrochloride;O-(2-methylprop-2-enyl)hydroxylamine;hydrochloride;O-(2-METHYL-ALLYL)-HYDROXYLAMINE HCL;O-(2-methylprop-2-en-1-yl)hydroxylamine hydrochloride;SCHEMBL3174913;DTXSID00500474;o-(2-methylallyl)hydroxylamine hcl;MFCD09838139;AKOS006327919;SB37586;DS-19523;O-(2-methylallyl)hydroxylaminehydrochloride;CS-0158063;EN300-260878;F31248;O-(2-Methylprop-2-en-1-yl)hydroxylamine--hydrogen chloride (1/1)

Chemical Property of O-(2-Methyl-allyl)-hydroxylamine hydrochloride

Chemical Property:

• PSA: 35.25000
• LogP: 1.95510
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 123.0450916
• Heavy Atom Count: 7
• Complexity: 51.5

Purity/Quality:

98% ^*data from raw suppliers

O-(2-Methylallyl)hydroxylaminehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)CON.Cl

Technology Process of O-(2-Methyl-allyl)-hydroxylamine hydrochloride

There total 1 articles about O-(2-Methyl-allyl)-hydroxylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-3-bromo-1-propene (1458-98-6) → O-(2-methylallyl)hydroxylamine hydrochloride (54149-64-3)

Guidance literature:

With hydroxylamine hydrochloride;

DOI:10.1055/s-2007-992373

Reference yield: 94.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + O-(2-methylallyl)hydroxylamine hydrochloride (54149-64-3) → cyclohexanone oxime O-methallyl ether (71350-17-9)

Guidance literature:

With sodium acetate; sodium carbonate; In ethanol; for 2h; Heating;

Reference yield: 74.0%

diethyl 2-formyl-1-phenylethylphosphonate (7749-92-0) + O-(2-methylallyl)hydroxylamine hydrochloride (54149-64-3) → C17H26NO4P (1012081-11-6)

Guidance literature:

With magnesium sulfate; triethylamine; In dichloromethane; at 20 ℃; for 15h;

DOI:10.1055/s-2007-992373

upstream raw materials:

2-methyl-3-bromo-1-propene

Downstream raw materials:

cyclohexanone oxime O-methallyl ether

C₁₇H₂₆NO₄P

Refernces