ba-D-arabino-2-Hexulopyranosidonic acid, methyl, methyl ester (9CI)

Base Information

• Chemical Name: ba-D-arabino-2-Hexulopyranosidonic acid, methyl, methyl ester (9CI)
• CAS No.: 528584-68-1
• Molecular Formula: C8H14O7
• Molecular Weight: 222.19
• Mol file: 528584-68-1.mol

Synonyms:bta-D-arabino-2-Hexulopyranosidonicacid,methyl,methylester(9CI);ba-D-arabino-2-Hexulopyranosidonic acid, methyl, methyl ester (9CI)

Chemical Property of ba-D-arabino-2-Hexulopyranosidonic acid, methyl, methyl ester (9CI)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ba-D-arabino-2-Hexulopyranosidonic acid, methyl, methyl ester (9CI)

There total 2 articles about ba-D-arabino-2-Hexulopyranosidonic acid, methyl, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2,2-dimethoxy-propane (77-76-9) + methyl β-L-sorbopyranoside (3765-95-5) → methyl (methyl β-L-sorbopyranoside)uronate (528584-68-1,528584-67-0)

Guidance literature:

methyl β-L-sorbopyranoside; With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hydrogencarbonate; sodium carbonate; In water; Electrochemical reaction;

With Amberlite IR 120; In water; for 0.5h;

2,2-dimethoxy-propane; With hydrogenchloride; In methanol; for 1h; Further stages.;

DOI:10.1002/ejoc.200390041

Reference yield: 54.0%

2,2-dimethoxy-propane (77-76-9) + methyl β-fructopyranoside (3765-95-5,4049-49-4,4208-77-9,15219-31-5,53685-18-0,60504-78-1,60504-80-5,60504-81-6,63526-48-7,79549-14-7,79549-15-8,79549-16-9,79549-17-0,143731-44-6) → methyl (methyl β-D-fructopyranoside)uronate (528584-68-1,528584-67-0)

Guidance literature:

methyl β-fructopyranoside; With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hydrogencarbonate; sodium carbonate; In water; Electrochemical reaction;

With Amberlite IR 120; In water; for 0.5h;

2,2-dimethoxy-propane; With hydrogenchloride; water; In methanol; for 1h; Further stages.;

DOI:10.1002/ejoc.200390041

upstream raw materials:

2,2-dimethoxy-propane

methyl β-fructopyranoside

methyl β-L-sorbopyranoside

Refernces