Technology Process of Thiazolidine, 2-(4-chlorophenyl)-3-(1-naphthalenylsulfonyl)- (9CI)
There total 4 articles about Thiazolidine, 2-(4-chlorophenyl)-3-(1-naphthalenylsulfonyl)- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(R)-AdDIP; sodium phosphate; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
In
toluene;
at 0 ℃;
for 48h;
Overall yield = 42%; enantioselective reaction;
DOI:10.1002/anie.201711277
- Guidance literature:
-
With
(R)-AdDIP; sodium phosphate; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
In
toluene;
at 0 ℃;
for 48h;
Overall yield = 42%; enantioselective reaction;
DOI:10.1002/anie.201711277
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / chloroform; water / 2 h / 20 °C
2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate; sodium phosphate; (R)-AdDIP / toluene / 48 h / 0 °C
With
(R)-AdDIP; sodium phosphate; sodium hydroxide; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
In
chloroform; water; toluene;
DOI:10.1002/anie.201711277