Technology Process of 1,2,3,5,6,7-Hexachloronaphthalene
There total 3 articles about 1,2,3,5,6,7-Hexachloronaphthalene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 1h;
Yield given. Yields of byproduct given;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 79 percent / sulfur monochloride, sulfuryl chloride, aluminium chloride / 5 h / Heating
2: 81 percent / diisopropyl ether / Heating
3: LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
With
lithium aluminium tetrahydride; aluminium trichloride; sulfuryl dichloride; sulfur monochloride;
In
tetrahydrofuran; di-isopropyl ether;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 81 percent / diisopropyl ether / Heating
2: LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; di-isopropyl ether;