Ethane-13C1

Base Information

• Chemical Name: Ethane-13C1
• CAS No.: 6145-17-1
• Molecular Formula: C2H6
• Molecular Weight: 31.0586
• European Community (EC) Number: 693-085-4
• DSSTox Substance ID: DTXSID50476559
• Nikkaji Number: J1.274.386F
• Mol file: 6145-17-1.mol

Synonyms:Ethane-13C1;6145-17-1;(113C)ethane;DTXSID50476559;Ethane-13C1, 99 atom % 13C;AKOS015913212

Chemical Property of Ethane-13C1

Chemical Property:

• Vapor Pressure: 37.95 atm ( 21.1 °C)
• Melting Point: −172 °C(lit.)
• Boiling Point: −88 °C(lit.)
• PSA: 0.00000
• Density: 1.05 (vs air)
• LogP: 1.02620
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 31.050305027
• Heavy Atom Count: 2
• Complexity: 0

Purity/Quality:

99% ^*data from raw suppliers

ETHANE-13C1 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F+
• Statements: 12
• Safety Statements: 16-33-38-9

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CC
• Isomeric SMILES: C[13CH3]

Technology Process of Ethane-13C1

There total 7 articles about Ethane-13C1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methane (6532-48-5) + propane (74-98-6) → ethane-13C1 (6145-17-1) + ethane (74-84-0) + ethane-13C2 (52026-74-1)

Guidance literature:

With tnatalum hydride on silica; at 250 ℃; Further Variations:; time dependence; Product distribution;

DOI:10.1002/anie.200460982

Reference yield:

ethanol-1-13C (14742-23-5) → carbon monoxide-13C-18O (35907-63-2) + carbon dioxide-13C-18O1 (20201-82-5) + methane (6532-48-5) + ethane-13C1 (6145-17-1) + methane (34557-54-5,27936-85-2) + ethane (74-84-0) + ethene (74-85-1) + ethane-13C2 (52026-74-1) + [13C2]ethene (51915-19-6) + mono-[13C]-ethylene (6145-18-2) + carbon dioxide (124-38-9,18923-20-1) + carbon monoxide (55125-78-5) + carbon dioxide (1111-72-4) + [13C]Carbon monoxide (1641-69-6) + carbon dioxide (2537-69-1) + CO(18)O (18983-82-9) + carbon dioxide (2684-00-6)

Guidance literature:

With ¹⁸O-labeled water; at 350 ℃; Reagent/catalyst; Inert atmosphere;

DOI:10.1002/anie.201604388

Reference yield:

ethanol-1-13C (14742-23-5) → carbon monoxide-13C-18O (35907-63-2) + carbon dioxide-13C-18O1 (20201-82-5) + methane (6532-48-5) + ethane-13C1 (6145-17-1) + methane (34557-54-5,27936-85-2) + ethane (74-84-0) + ethene (74-85-1) + ethane-13C2 (52026-74-1) + [13C2]ethene (51915-19-6) + mono-[13C]-ethylene (6145-18-2) + carbon monoxide (55125-78-5) + carbon dioxide (1111-72-4) + [13C]Carbon monoxide (1641-69-6) + carbon dioxide (2537-69-1) + CO(18)O (18983-82-9) + carbon dioxide (2684-00-6)

Guidance literature:

With ¹⁸O-labeled water; at 350 ℃; Inert atmosphere;

DOI:10.1002/anie.201604388

upstream raw materials:

(5-⁽¹³⁾C)n-nonane

¹³C-2-propane

methane

ethane

Downstream raw materials:

methane

methane

propane

2,2-dimethylpropane

Refernces

• 1、 Soulivong, Daravong,Coperet, Christophe,Thivolle-Cazat, Jean,Basset, Jean-Marie,Maunders, Barry M.,Pardy, Richard B. A.,Sunley, Glenn J.. "Cross-metathesis of propane and methane: A catalytic reaction of C-C bond cleavage of a higher alkane by methane". . p. 5366 - 5369. Retrieved 2007/10/03.
• 2、 Weeks, Thomas J.,Ladd, Irwin R.,Bolton, Anthony P.. "Cracking of (5-(13)C)-n-Nonane with Quartz Wool, Silica-Alumina and Type Y Zeolite". . p. 84 - 91. Retrieved 2007/10/02.