HEXATETRACONTANE

Base Information

• Chemical Name: HEXATETRACONTANE
• CAS No.: 7098-24-0
• Molecular Formula: C46H94
• Molecular Weight: 647.24
• Mol file: 7098-24-0.mol

Synonyms:HEXATETRACONTANE;ALKANE C46;N-HEXATETRACONTANE;HEXATETRACONTANE, STANDARD FOR GC

Chemical Property of HEXATETRACONTANE

Chemical Property:

• Vapor Pressure: 6.25E-12mmHg at 25°C
• Melting Point: 86-89 °C
• Refractive Index: 1.458
• Boiling Point: 558.4°C at 760 mmHg
• Flash Point: 468.1°C
• PSA: 0.00000
• Density: 0.821g/cm³
• LogP: 18.19060

Purity/Quality:

98%Min ^*data from raw suppliers

Hexatetracontane analytical standard ^*data from reagent suppliers

Safty Information:

• Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of HEXATETRACONTANE

There total 5 articles about HEXATETRACONTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

C52H102S4 (448261-28-7) → hexatetracontane (7098-24-0)

Guidance literature:

With nickel; In cyclohexane; for 2h; Heating;

DOI:10.1271/bbb.66.523

Reference yield:

1,12-dibromododecane (3344-70-5) → hexatetracontane (7098-24-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 79 percent / buthyllithium / tetrahydrofuran; hexane / -45 - -10 °C

2: 50 percent / butyllithium / tetrahydrofuran; hexane / -15 - -10 °C

3: 40 percent / butyllithium / tetrahydrofuran; hexane / -15 - -10 °C

4: 79 percent / Raney nickel / cyclohexane / 2 h / Heating

With n-butyllithium; nickel; In tetrahydrofuran; hexane; cyclohexane;

DOI:10.1271/bbb.66.523

Reference yield:

C20H38S4 (448260-82-0) → hexatetracontane (7098-24-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 50 percent / butyllithium / tetrahydrofuran; hexane / -15 - -10 °C

2: 40 percent / butyllithium / tetrahydrofuran; hexane / -15 - -10 °C

3: 79 percent / Raney nickel / cyclohexane / 2 h / Heating

With n-butyllithium; nickel; In tetrahydrofuran; hexane; cyclohexane;

DOI:10.1271/bbb.66.523

upstream raw materials:

1-bromotricosane

C₅₂H₁₀₂S₄

1,12-dibromododecane

C₂₀H₃₈S₄

Refernces