ACETONE-1,3-13C2

Base Information

• Chemical Name: ACETONE-1,3-13C2
• CAS No.: 7217-25-6
• Molecular Formula: C3H6O
• Molecular Weight: 60.058
• Mol file: 7217-25-6.mol

Synonyms:ACETONE-1,3-13C2;ACETONE-1,3-13C2, 99 ATOM % 13C

Chemical Property of ACETONE-1,3-13C2

Chemical Property:

• Vapor Pressure: 184 mm Hg ( 20 °C)
• Melting Point: -94 °C(lit.)
• Refractive Index: n20/D 1.359(lit.)
• Boiling Point: 56 °C(lit.)
• Flash Point: 1 °F
• PSA: 17.07000
• Density: 0.818 g/mL at 25 °C
• LogP: 0.59530

Purity/Quality:

98% ^*data from raw suppliers

Acetone-1,3-13C2 99 atom % ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,Xi
• Statements: 11-67-66-36
• Safety Statements: 9-16-23-33-26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of ACETONE-1,3-13C2

There total 1 articles about ACETONE-1,3-13C2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-13C)acetic acid (1563-80-0) → [1,3-13C2]-acetone (7217-25-6) + carbon dioxide (124-38-9,18923-20-1) + (1,3,3-<13C>3)-2-methylpropene

Guidance literature:

With Zn₂Zr₈O(x); at 449.84 ℃;

DOI:10.1021/cs501018k

Reference yield: 99.0%

[1,3-13C2]-acetone (7217-25-6) + trisylhydrazine (39085-59-1) → [1,3-13C2]acetone-2,4,6-tri-isopropylbenzenesulphonylhydrazone

Guidance literature:

In methanol; at 20 ℃; for 0.75h;

DOI:10.1016/S0039-128X(99)00102-6

Reference yield: 63.0%

[1,3-13C2]-acetone (7217-25-6) + nitromalondialdehyde sodium salt (34461-00-2) → [2,6-13C2]4-nitrophenol (70479-88-8)

Guidance literature:

With sodium hydroxide; In water; at 0 - 4 ℃; for 144h;

DOI:10.1039/c4ob01129e

upstream raw materials:

(2-¹³C)acetic acid

Downstream raw materials:

[2,6-¹³C₂]4-nitrophenol

carbon dioxide

Refernces