DIALLYLFORMAL

Base Information

• Chemical Name: DIALLYLFORMAL
• CAS No.: 7426-81-5
• Molecular Formula: C9H16O2
• Molecular Weight: 128.171
• Mol file: 7426-81-5.mol

Synonyms:DIALLYLFORMAL;FORMALDEHYDE DIALLYL ACETAL

Chemical Property of DIALLYLFORMAL

Chemical Property:

• Vapor Pressure: 8.75mmHg at 25°C
• Refractive Index: 1.422
• Boiling Point: 137.4°C at 760 mmHg
• Flash Point: 29.1°C
• PSA: 18.46000
• Density: 0.871g/cm³
• LogP: 1.34910

Purity/Quality:

98%Min ^*data from raw suppliers

DIALLYLFORMAL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of DIALLYLFORMAL

There total 6 articles about DIALLYLFORMAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.8%

allyl alcohol (107-18-6) + 1,1-dibromomethane (74-95-3) → bis(allyloxy)methane (7426-81-5)

Guidance literature:

With sodium hydride; Heating;

Reference yield:

allyl alcohol (107-18-6) + allyl chloromethyl ether (3970-20-5) → bis(allyloxy)methane (7426-81-5)

Guidance literature:

With pyridine;

DOI:10.1021/ja01140a039

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + allyl alcohol (107-18-6) → bis(allyloxy)methane (7426-81-5)

Guidance literature:

With calcium chloride; In benzene;

DOI:10.1039/jr9620004307

upstream raw materials:

allyl alcohol

allyl chloromethyl ether

formaldehyd

1,1-dibromomethane

Downstream raw materials:

diphenyl <(allyloxy)methyl>phosphonate

(+/-)-tetrahydrofuran-3-yl acetate

1,2,4-trihydroxybutane triacetate

5-ethyl-6-{3-[(5-ethyl-1-allyloxymethyl-2,6-dioxopyrimidin-4(1H,3H)-yl)methyl]benzyl}pyrimidine-2,4(1H,3H)-dione

Refernces

• 1、 El-Brollosy, Nasser R.. "Synthesis and antimicrobial evaluation of 6-azauracil non-nucleosides". scheme or table. p. 1483 - 1490. Retrieved 2009/12/26.
• 2、 El-Brollosy, Nasser R.,J?rgensen, Per T.,Dahan, Berit,Boel, Anne Marie,Pedersen, Erik B.,Nielsen, Claus. "Synthesis of novel N-1 (allyloxymethyl) analogues of 6-benzyl-1-(ethoxymethyl)-5-isopropyluracil (MKC-442, emivirine) with improved activity against HIV-1 and its mutants". . p. 5721 - 5726. Retrieved 2007/10/03.