Technology Process of 14-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane
There total 5 articles about 14-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
methanol; water;
at 25 ℃;
for 0.1h;
Yield given;
Irradiation;
other solvent: o-dichlorobenzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorus oxychloride
2: 2.) water / 1.) benzene, reflux, 60 h, 2.) 48 h
3: methanol; H2O / 0.1 h / 25 °C / Irradiation; other solvent: o-dichlorobenzene
With
water; trichlorophosphate;
In
methanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) sodium nitrite, hydrochloric acid, 2.) sodium hydroxide, sodium sulfate / 2.) water, 24 h
2: 2.) water / 1.) benzene, reflux, 60 h, 2.) 48 h
3: methanol; H2O / 0.1 h / 25 °C / Irradiation; other solvent: o-dichlorobenzene
With
hydrogenchloride; sodium hydroxide; water; sodium sulfate; sodium nitrite;
In
methanol; water;