Chromium, bis(1,3-di(trifluoromethyl)benzene)-

Base Information

• Chemical Name: Chromium, bis(1,3-di(trifluoromethyl)benzene)-
• CAS No.: 53966-05-5
• Molecular Formula: C₁₆H₈CrF₁₂
• Molecular Weight: 480.216
• Mol file: 53966-05-5.mol

Synonyms:Chromium, bis(1,3-di(trifluoromethyl)benzene)-;QBUPRWAGKHACKR-UHFFFAOYSA-N;53966-05-5

Chemical Property of Chromium, bis(1,3-di(trifluoromethyl)benzene)-

Chemical Property:

• Vapor Pressure: 22.1mmHg at 25°C
• Boiling Point: 116°C at 760 mmHg
• Flash Point: 26.1°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 18
• Rotatable Bond Count: 0
• Exact Mass: 479.983943
• Heavy Atom Count: 29
• Complexity: 514

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: [CH-]1[CH-][C-]([CH-][C-]([CH-]1)C(F)(F)F)C(F)(F)F.C1=CC(=CC(=C1)C(F)(F)F)C(F)(F)F.[Cr]

Technology Process of Chromium, bis(1,3-di(trifluoromethyl)benzene)-

There total 1 articles about Chromium, bis(1,3-di(trifluoromethyl)benzene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromobenzene (108-86-1,52753-63-6) + 1,3-bis(trifluoromethyl)benzene (402-31-3) + chromium (7440-47-3) → (m-(CF3)2C6H4)2Cr (53966-05-5) + Cr(C6H5Br)(C6H4(CF3)2-1,3) (163089-95-0)

Guidance literature:

In neat (no solvent); condensation at -196°C of Cr vapor (obtained by heating of solid)with equimolar mixt. of arenes; evapn. (reduced pressure), dissoln. in hexane at room temp., evapn., sublimation (vac.); product mixt. not sepd., detd. by mass spectroscopy;

DOI:10.1016/0022-328X(94)05104-J

upstream raw materials:

bromobenzene

1,3-bis(trifluoromethyl)benzene

chromium

Refernces