Sn(C₆H₅)2(C₅H₅)OOCC₆H₄Cl

Base Information

• Chemical Name: Sn(C₆H₅)2(C₅H₅)OOCC₆H₄Cl
• CAS No.: 132608-92-5
• Molecular Formula: C₂₄H₁₉ClO₂Sn
• Molecular Weight: 493.577
• Mol file: 132608-92-5.mol

Synonyms:

Chemical Property of Sn(C₆H₅)2(C₅H₅)OOCC₆H₄Cl

Chemical Property:

Purity/Quality:

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Technology Process of Sn(C₆H₅)2(C₅H₅)OOCC₆H₄Cl

There total 1 articles about Sn(C₆H₅)2(C₅H₅)OOCC₆H₄Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

diphenylcyclopentadienyltin chloride (54599-88-1) + silver(I) 4-chlorobenzoate (72247-98-4) → Sn(C6H5)2(C5H5)OOCC6H4Cl (132608-92-5)

Guidance literature:

In tetrahydrofuran; byproducts: AgCl; (N2); dropwise addn. of Sn(C6H5)2(C5H5)Cl soln. to suspn. of silver carboxylate at 0°C with stirring; further stirring for 3 h; removal of AgCl by filtration; filtrate concg.; addn. of petroleum ether (60-80°C); washing (petroleum ether); drying in vac.; elem. anal.;

upstream raw materials:

diphenylcyclopentadienyltin chloride

silver(I) 4-chlorobenzoate

Refernces