La(C₁₅H₁₃N₄S)Cl₂

Base Information

• Chemical Name: La(C₁₅H₁₃N₄S)Cl₂
• CAS No.: 262291-32-7
• Molecular Formula: C₁₅H₁₃Cl₂LaN₄S
• Molecular Weight: 491.173
• Mol file: 262291-32-7.mol

Synonyms:

Chemical Property of La(C₁₅H₁₃N₄S)Cl₂

Chemical Property:

Purity/Quality:

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Technology Process of La(C₁₅H₁₃N₄S)Cl₂

There total 1 articles about La(C₁₅H₁₃N₄S)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

dibenzylidenethiocarbohydrazide (6956-33-8) + lanthanum(III) chloride (10099-58-8) → La(C15H13N4S)Cl2 (262291-32-7)

Guidance literature:

With potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide; byproducts: HCl; the ligand was added to a refluxing DMF-EtOH soln. (1:1) of LaCl3, followed by the addn. of an aq. ethanolic soln. of KOH, the mixt. was refluxed for 10 h, cooled to room temp.; Et2O was added, allowed to stand for 5-6 h, ppt. was filtered, washed with water and ether and recrystd. from DMF-Et2O-EtOH and dried in vac.; elem. anal.;

DOI:10.1080/00945710009351753

upstream raw materials:

dibenzylidenethiocarbohydrazide

lanthanum(III) chloride

Refernces