Technology Process of sodium 2-(1-adamantyloxy)ethyl (p-tosyloxy)methylphosphonate
There total 5 articles about sodium 2-(1-adamantyloxy)ethyl (p-tosyloxy)methylphosphonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 6.75 h / 0 - 20 °C
2: pyridine / diethyl ether
3: water; sodium hydrogencarbonate
With
pyridine; oxalyl dichloride; water; sodium hydrogencarbonate; N,N-dimethyl-formamide;
In
diethyl ether; dichloromethane;
DOI:10.1134/S1070363209080313
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dichloromethane / 16 h
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 6.75 h / 0 - 20 °C
3: pyridine / diethyl ether
4: water; sodium hydrogencarbonate
With
pyridine; oxalyl dichloride; water; sodium hydrogencarbonate; N,N-dimethyl-formamide;
In
diethyl ether; dichloromethane;
DOI:10.1134/S1070363209080313
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine / 5 h / 110 °C
2: pyridine / diethyl ether
3: water; sodium hydrogencarbonate
With
pyridine; water; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
diethyl ether;
DOI:10.1134/S1070363209080313
