dihydro-13(S),17,22,23-tetramethoxylythran-11-one

Base Information

• Chemical Name: dihydro-13(S),17,22,23-tetramethoxylythran-11-one
• CAS No.: 76193-24-3
• Molecular Formula: C₂₈H₃₅NO₆
• Molecular Weight: 481.589
• Mol file: 76193-24-3.mol

Synonyms:

Chemical Property of dihydro-13(S),17,22,23-tetramethoxylythran-11-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dihydro-13(S),17,22,23-tetramethoxylythran-11-one

There total 1 articles about dihydro-13(S),17,22,23-tetramethoxylythran-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-lythrine (10308-13-1,57572-82-4,57572-83-5,5286-10-2) → dihydro-13(S),17,22,23-tetramethoxylythran-11-one (76193-24-3,76193-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) mercuric acetate, 2.) sodium borohydride / 1.) 3 d, room temp.

2: 67 percent / 10percent sodium hydroxide / dioxane

With sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate; In 1,4-dioxane;

DOI:10.1139/v80-291

upstream raw materials:

(+)-lythrine

Refernces