2,3-dibromopropyl acetate

Base Information

• Chemical Name: 2,3-dibromopropyl acetate
• CAS No.: 6308-13-0
• Molecular Formula: C5H8 Br2 O2
• Molecular Weight: 259.925
• Mol file: 6308-13-0.mol

Synonyms:1-Propanol,2,3-dibromo-, acetate (6CI,7CI,8CI,9CI); 1,2-Dibromo-3-acetoxypropane;2,3-Dibromopropanyl acetate; 2,3-Dibromopropyl acetate; NSC 43369

Chemical Property of 2,3-dibromopropyl acetate

Chemical Property:

• Vapor Pressure: 0.0105mmHg at 25°C
• Boiling Point: 263.1°C at 760 mmHg
• Flash Point: 112.9°C
• Density: 1.839g/cm³

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dibromopropyl acetate

There total 7 articles about 2,3-dibromopropyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

2,3-Dibromopropan-1-ol (96-13-9) + acetic acid (64-19-7,77671-22-8) → 1-acetoxy-2,3-dibromopropane (6308-13-0)

Guidance literature:

With sulfuric acid; at 90 ℃; for 24h;

Reference yield:

Allyl acetate (591-87-7) + N-bromobenzamide (19964-97-7) → 1-acetoxy-2,3-dibromopropane (6308-13-0)

Guidance literature:

With tetrachloromethane;

DOI:10.1021/jo01085a001

Reference yield:

Allyl acetate (591-87-7) → 1-acetoxy-2,3-dibromopropane (6308-13-0)

Guidance literature:

With diethyl ether; bromine;

upstream raw materials:

Allyl acetate

N-bromobenzamide

2,3-Dibromopropan-1-ol

acetyl chloride

Downstream raw materials:

1,2-Epoxy-3-bromopropane

triacetylglycerol

Refernces

• 1、 Loepez, Anna,Moreno-Manas, Marcial,Pleixats, Roser,Roglans, Anna. "Pd(0)-based synthetic approaches to 1,1-disubstituted-3,4-dimethylenecyclopentanes as intermediates in the preparation of a,a-disubstituted amino acid derivatives possessing indane and diazaindane skeletons". . p. 355 - 362. Retrieved 2007/10/03.