chrysen-6-yl-o-tolyl ketone

Base Information

• Chemical Name: chrysen-6-yl-o-tolyl ketone
• CAS No.: 115534-81-1
• Molecular Formula: C₂₆H₁₈O
• Molecular Weight: 346.428
• Mol file: 115534-81-1.mol

Synonyms:

Chemical Property of chrysen-6-yl-o-tolyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chrysen-6-yl-o-tolyl ketone

There total 2 articles about chrysen-6-yl-o-tolyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chrysene (218-01-9) + ortho-toluoyl chloride (933-88-0) → chrysen-6-yl-o-tolyl ketone (115534-81-1)

Guidance literature:

With aluminium trichloride; In carbon disulfide; Heating;

DOI:10.1021/jo01077a006

Reference yield:

2-methylchlorobenzene (95-49-8) + chrysene (218-01-9) → chrysen-6-yl-o-tolyl ketone (115534-81-1)

Guidance literature:

With aluminium trichloride;

DOI:10.1021/jo01077a006 DOI:10.1039/jr9570004163

Reference yield:

chrysen-6-yl-o-tolyl ketone (115534-81-1) → 12-Amino-6-o-toluoyl-chrysen (96674-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: HNO₃, H₂SO₄ / acetic acid

2: N₂H₄*H₂O, KOH / bis-(2-hydroxy-ethyl) ether

With potassium hydroxide; sulfuric acid; nitric acid; hydrazine hydrate; In acetic acid; diethylene glycol;

upstream raw materials:

2-methylchlorobenzene

chrysene

ortho-toluoyl chloride

Downstream raw materials:

1,2,5,6-Dibenzo-tetraphen

12-Amino-6-o-toluoyl-chrysen