potassium 1,2-propanediaminetriacetatoacetic acid nickelate(II) monohydrate

Base Information

• Chemical Name: potassium 1,2-propanediaminetriacetatoacetic acid nickelate(II) monohydrate
• CAS No.: 117849-66-8
• Molecular Formula: C₁₁H₁₄N₂O₈*H*H₂O*K*Ni
• Molecular Weight: 419.052
• Mol file: 117849-66-8.mol

Synonyms:

Chemical Property of potassium 1,2-propanediaminetriacetatoacetic acid nickelate(II) monohydrate

Chemical Property:

Purity/Quality:

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Technology Process of potassium 1,2-propanediaminetriacetatoacetic acid nickelate(II) monohydrate

There total 1 articles about potassium 1,2-propanediaminetriacetatoacetic acid nickelate(II) monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.7%

nickel(II) iodide (13462-90-3) + 1,2-diaminopropane-N,N,N',N'-tetraacetic acid (4408-81-5) → potassium 1,2-propanediaminetriacetatoacetic acid nickelate(II) monohydrate (117849-66-8,116122-67-9,117893-78-4)

Guidance literature:

With potassium hydroxide; In ethanol; water; warm soln. of K2H2PDTA (racemic)(ethanol/water) dropped into NiI2 soln. (ethanol, stirring); filtrate dropped into ice cold abs. ethanol, slurry centrifuged several times until no yellow filtrate; ppt. washed with acetone, air dried and ground; powder dissolved in H2O; CCl4 and H2O2 (30 %) added; shaking ; CCl4 layer discarded, procedure repeated several times ; aq. layer filtered into cold ethanol; repptn. in refrigerator;ppt. washed with ethanol and acetone, air dried (vac.); elem. anal.;

upstream raw materials:

nickel(II) iodide

1,2-diaminopropane-N,N,N',N'-tetraacetic acid