dibromobis(triphenylphosphine)nickel(II)

Base Information Edit

Chemical Name:dibromobis(triphenylphosphine)nickel(II)
CAS No.:36673-36-6
Molecular Formula:C₃₆H₃₀Br₂NiP₂
Molecular Weight:743.08
Hs Code.:
Mol file:36673-36-6.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibromobis(triphenylphosphine)nickel(II) Edit

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Technology Process of dibromobis(triphenylphosphine)nickel(II)

There total 25 articles about dibromobis(triphenylphosphine)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 23777-40-4
bis(triphenylphosphine)ethylenenickel⁽⁰⁾

: 91-13-4
α,α'-dibromo-o-xylene

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

: 1460-59-9
5,6,11,12-tetrahydro-dibenzo[a,e]cyclooctene

Guidance literature:: In diethyl ether; under Ar, into stirred soln. of C6H4(CH2Br)2 in ether Ni complex introduced at -20°C over 1 h;
DOI:10.1016/S0022-328X(00)83863-2

Reference yield: 90.0%

: 603-35-0
triphenylphosphine

: 13462-88-9
nickel dibromide

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

Guidance literature:: In ethanol; (N2), NiBr2 refluxed with PPh3 in dry EtOH; hot filtered, cooled. crystd., filtered, dried (vac.), elem. anal.;
DOI:10.1016/j.molcata.2005.12.027

Reference yield: 89.0%

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 590-17-0
cyanomethyl bromide

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

Guidance literature:: With P(C₆H₅)3; In toluene; (Ar); to a soln. of Ni(COD)2 Ph3P is added, to this mixt. BrCH2CN is added; pptn with n-hexane, ppt. is filtered off, washed with n-hexane, elem. anal.;