dinitrato[2,3:9,10-biphenyldiamine-5,7,12,14-tetramethyl-1,4,8,11-tetraazacycloteradecane-4,7,11,14-tetraene]cobalt(II)

Base Information

• Chemical Name: dinitrato[2,3:9,10-biphenyldiamine-5,7,12,14-tetramethyl-1,4,8,11-tetraazacycloteradecane-4,7,11,14-tetraene]cobalt(II)
• CAS No.: 1338990-02-5
• Molecular Formula: C₃₄H₃₆CoN₁₀O₆
• Molecular Weight: 739.716
• Mol file: 1338990-02-5.mol

Synonyms:

Chemical Property of dinitrato[2,3:9,10-biphenyldiamine-5,7,12,14-tetramethyl-1,4,8,11-tetraazacycloteradecane-4,7,11,14-tetraene]cobalt(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dinitrato[2,3:9,10-biphenyldiamine-5,7,12,14-tetramethyl-1,4,8,11-tetraazacycloteradecane-4,7,11,14-tetraene]cobalt(II)

There total 1 articles about dinitrato[2,3:9,10-biphenyldiamine-5,7,12,14-tetramethyl-1,4,8,11-tetraazacycloteradecane-4,7,11,14-tetraene]cobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

3,3',4,4'-tetraaminobiphenyl (91-95-2) + cobalt(II) nitrate hexahydrate + acetylacetone (123-54-6,81235-32-7) → dinitrato[2,3:9,10-biphenyldiamine-5,7,12,14-tetramethyl-1,4,8,11-tetraazacycloteradecane-4,7,11,14-tetraene]cobalt(II) (1338990-02-5)

Guidance literature:

In water; acetonitrile; to soln. (CH3CN:distd. H2O 1:1) of diaminobenzidine placed in round-bottom flask slowly added soln. (CH3CN) of acetylacetone, stirred for about 2-3 h, added soln. (CH3CN) of Co(NO3)2, stirred for 12 h; solid filtered, washed with methanol, dried (vac.); elem. anal.;

DOI:10.1080/15533174.2011.591345

upstream raw materials:

3,3',4,4'-tetraaminobiphenyl

acetylacetone

Refernces