Technology Process of 1-chloro-1-phenoxy-2-n-butylcyclopropane
There total 5 articles about 1-chloro-1-phenoxy-2-n-butylcyclopropane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
pentane;
at 25 ℃;
for 72h;
sealed tube, in the dark;
DOI:10.1021/jo00143a001
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 47 percent / aq. NaOH / H2O / 1.) 13 deg C, 30 min, 2.) 25 deg C, 45 min
2: 37 percent / LiCl, DMSO, satd. aq. NaCl in 11percent aq. NaOCl / pentane / 0.83 h / -5 °C
3: 10 percent / pentane / 72 h / 25 °C / sealed tube, in the dark
With
sodium hydroxide; sodium hypochlorite; dimethyl sulfoxide; lithium chloride; sodium chloride;
In
water; pentane;
DOI:10.1021/jo00143a001
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 37 percent / LiCl, DMSO, satd. aq. NaCl in 11percent aq. NaOCl / pentane / 0.83 h / -5 °C
2: 10 percent / pentane / 72 h / 25 °C / sealed tube, in the dark
With
sodium hypochlorite; dimethyl sulfoxide; lithium chloride; sodium chloride;
In
pentane;
DOI:10.1021/jo00143a001
