(S)-9-hydroxystearic acid palmitic acid ester

Base Information

• Chemical Name: (S)-9-hydroxystearic acid palmitic acid ester
• CAS No.: 2097130-84-0
• Molecular Formula: C₃₄H₆₆O₄
• Molecular Weight: 538.896
• Mol file: 2097130-84-0.mol

Synonyms:

Chemical Property of (S)-9-hydroxystearic acid palmitic acid ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-9-hydroxystearic acid palmitic acid ester

There total 42 articles about (S)-9-hydroxystearic acid palmitic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl 9-(palmitoyloxy)octadecanoate → 9-PAHSA (2097130-84-0,2097130-87-3)

Guidance literature:

With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 0 - 23 ℃; for 12h;

DOI:10.1038/s41429-019-0180-1

Reference yield: 88.0%

(S)-1-hydroxyoctadecan-9-yl palmitate → (S)-9-hydroxystearic acid palmitic acid ester (2097130-84-0,2097130-87-3)

Guidance literature:

With Jones reagent; In acetone; at 0 ℃; for 1h;

DOI:10.1002/ejoc.201801881

Reference yield: 53.0%

C26H41BrO4 + n-hexadecanoyl chloride (112-67-4) → 9-PAHSA (2097130-84-0,2097130-87-3)

Guidance literature:

C₂₆H₄₁BrO₄; n-hexadecanoyl chloride; With dmap;

With acetic acid; zinc;

upstream raw materials:

9-hydroxystearic acid

n-hexadecanoyl chloride

1,9-Nonanediol

9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol

Refernces

• 1、 Guin, Joyram,Paul, Subhasis. "A General Approach to Intermolecular Olefin Hydroacylation through Light-Induced HAT Initiation: An Efficient Synthesis of Long-Chain Aliphatic Ketones and Functionalized Fatty Acids". . p. 4412 - 4419. Retrieved 2021/02/05.
• 2、 Mountanea, Olga G.,Limnios, Dimitris,Kokotou, Maroula G.,Bourboula, Asimina,Kokotos, George. "Asymmetric Synthesis of Saturated Hydroxy Fatty Acids and Fatty Acid Esters of Hydroxy Fatty Acids". . p. 2010 - 2019. Retrieved 2019/03/07.