Technology Process of 3'-Desoxyribostamycin
There total 9 articles about 3'-Desoxyribostamycin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
water;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/acs.jmedchem.6b00793
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triflic azide; zinc(II) chloride / dichloromethane; methanol; water / Inert atmosphere
2: pyridine / 6 h / 20 °C
3: boron trifluoride diethyl etherate / dichloromethane / -50 °C / Inert atmosphere; Molecular sieve
4: potassium carbonate; methanol / dichloromethane / 20 °C / Inert atmosphere
5: palladium 10% on activated carbon; hydrogen / water / 3 h / 20 °C / Inert atmosphere
With
pyridine; methanol; triflic azide; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; potassium carbonate; zinc(II) chloride;
In
methanol; dichloromethane; water;
DOI:10.1021/acs.jmedchem.6b00793
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / 6 h / 20 °C
2: boron trifluoride diethyl etherate / dichloromethane / -50 °C / Inert atmosphere; Molecular sieve
3: potassium carbonate; methanol / dichloromethane / 20 °C / Inert atmosphere
4: palladium 10% on activated carbon; hydrogen / water / 3 h / 20 °C / Inert atmosphere
With
pyridine; methanol; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; potassium carbonate;
In
dichloromethane; water;
DOI:10.1021/acs.jmedchem.6b00793
